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1 article(s) from Gruß, Hendrik

Peptide stapling by late-stage Suzuki–Miyaura cross-coupling

Hendrik Gruß,
Rebecca C. Feiner,
Ridhiwan Mseya,
David C. Schröder,
Michał Jewgiński,
Kristian M. Müller,
Rafał Latajka,
Antoine Marion and
Norbert Sewald

Beilstein J. Org. Chem. 2022, 18, 1–12, doi:10.3762/bjoc.18.1

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Scheme 1: Synthesis of SMC stapled axin CBD peptides. Reaction conditions: (a) Pd₂(dba)₃, sSPhos, KF, DME/EtO...

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Scheme 2: Overview of the different cross-linkages obtained by intramolecular SMC. A) General structure of SM...

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Figure 1: Analysis of the secondary structure by circular dichroism: CD spectra of both isomers of stapled pe...

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Figure 2: In vitro binding affinities to β-catenin determined by competitive fluorescence polarisation assays....

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Figure 3: Cleavage sites of Proteinase K digestion indicated by a red arrow.

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Figure 4: Principal component analysis (PCA) of the macrocycle’s non-hydrogen atoms in the two isomers of P5....

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Figure 5: Molecular modelling of the conformational preferences of the SMC stapled peptides P5 (with cis or t...

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Published 03 Jan 2022

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